46 C.F.R. Subpart 54.05—Toughness Tests


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PART 54—PRESSURE VESSELS

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Subpart 54.05—Toughness Tests

§ 54.05-1   Scope (replaces UG–84).

(a) The toughness tests of materials used in pressure vessels shall be as required by this subpart in lieu of requirements in UG–84 of the ASME Code.

§ 54.05-3   Tests required.

(a) Where material or welding toughness tests are required by §§54.25–10, 54.25–15, 54.25–20, and subpart 57.03 or 57.06 of this subchapter, the following requirements shall apply:

(1) Additional requirements for ferritic steels with properties enhanced by heat treatment are in §54.25–20.

(2) Certified reports of toughness tests by the material manufacturer will be acceptable evidence provided the specimens taken are representative of the material delivered and that the material is not subject to treatment during or following fabrication that will reduce its impact properties. If such treatment is subsequently applied to the material, test specimens shall be so taken and treated as to be representative of the material in the finished vessel.

(b) The requirements of this subpart are also applicable to nonpressure vessel type low temperature tanks and associated secondary barriers, as defined in §38.05–4 of subchapter D (Tank Vessels) of this chapter.

[CGFR 68–82, 33 FR 18828, Dec. 18, 1968, as amended by CGFR 69–127, 35 FR 9977, June 17, 1970]

§ 54.05-5   Toughness test specimens.

(a) Charpy V-notch impact tests. Where required, Charpy V-notch tests shall be conducted in accordance with ASTM Specification E 23 (incorporated by reference, see §54.01–1), “Notched Bar Impact Testing of Metallic Materials”, using the Type A specimen shown in Figure 4 of the specification. Special attention is drawn to the fact that the Charpy Keyhole and U-notch specimens are not acceptable substitutes for the Charpy V-notch specimen and shall not be used to qualify materials within the scope of this subpart. Each set of Charpy impact tests shall consist of three specimens. For materials 1/2-inch thick or less, the largest possible Charpy specimens for that thickness shall be cut centered at the material's mid-thickness. For materials thicker than 1/2-inch, full size Charpy specimens shall be cut centered at a location as near as practicable to a point midway between the material's surface and half-thickness. Except where otherwise specified, transversely oriented specimens must be used. When longitudinal specimens are used, the required energy values may not be less than 1.5 times the values required for transversely oriented specimens. In all cases the notch shall be cut normal to the material's surface. Test specimens shall be taken at least one “t” from any heat treated edge (where “t” is the material's nominal thickness).

(b) Drop weight tests. Where required, drop weight tests shall be conducted for no-break performance in accordance with ASTM Specification E 208 (incorporated by reference, see §54.01–1), “Conducting Drop-Weight Test to Determine Nil-Ductility Transition Temperature of Ferritic Steels”. For material thicknesses between 1/2-inch and 5/8-inch, the ASTM E–208 specimen P–3, machined to 1/2-inch thickness, shall be used with a stop distance of 0.090–inch. In preparing weld specimens for dropweight testing, weld reinforcement shall be ground flush, the hard facing bead centered on and transverse to the weld, and the notch centered on and parallel to the weld axis.

(c) Retest procedures. (1) When Charpy V-notch impact specimens are used and the average value of the three initial specimens fails to meet the stated requirements by an amount not exceeding 15 percent, or the value for more than one specimen is below the required average value of when the value for one specimen is below the minimum value permitted for a single specimen by an amount not exceeding 15 percent, three additional specimens from the same material may be tested and the results combined with those previously obtained to form a new average. This new average of six specimens must exceed the specified minimum average. In the event the Charpy retests fail, the material may still be qualified by exhibiting a no-break performance when tested in accordance with the drop weight procedure, if applicable. Two drop weight specimens shall be tested for each Charpy V-notch set of three initial specimens which failed to qualify. Failure of either or both of these drop weight specimens will constitute rejection of the material or weldments represented, except as outlined in paragraph (c)(3) of this section.

(2) When drop weight specimens are used, retests shall be permitted only within the limits prescribed in ASTM Specification E 208 (incorporated by reference, see §54.01–1), except as outlined in paragraph (c)(3) of this section.

(3) If, for heat treated base material, the required toughness results are not obtained in the initial test or in the retest, the material may be reheat treated one time and tested again in accordance with the initial requirements for the material.

(d) Alternate toughness tests. The Charpy V-notch impact values of §§54.05–20(a) and 54.05–25(a) are representative of those which correlate with the nil-ductility transition temperature determined by the drop-weight tests for the steels specified in §54.25–10. For materials for which there are other data showing suitable correlation between Charpy V-notch and drop-weight tests, V-notch acceptance limits different from those tabulated herein may be specially approved by the Commandant, based upon the actual correlation. In the case of steels for which the tabulated Charpy V-notch values can be shown to be inapplicable or in the case of specially considered steels, or as an alternative to complying with the tabulated impact requirements, acceptance may be based upon the material exhibiting a no-break performance when tested in accordance with the drop-weight procedure. Whenever the drop-weight test is used as an alternative to the Charpy V-notch test, two drop-weight specimens shall be tested for each set of three Charpy V-notch specimens otherwise required. If the drop-weight test cannot be performed because of material thickness limitations (less than one-half inch) or product shape, or is otherwise inapplicable (because of heat treatment, chemistry, etc.), other tests and/or test criteria will be specified by the Commandant to assure the adequacy of the material for the intended application.

[CGFR 68–82, 33 FR 18828, Dec. 18, 1968, as amended by CGD 73–254, 40 FR 40163, Sept. 2, 1975; USCG–2000–7790, 65 FR 58460, Sept. 29, 2000]

§ 54.05-6   Toughness test temperatures.

Each toughness test must be conducted at temperatures not warmer than −20 °F or 10 °F below the minimum service temperature, whichever is lower, except that for service at or below −320 °F, the tests may be conducted at the service temperature in accordance with §54.25–10(a)(2).

[CGD 85–061, 54 FR 50964, Dec. 11, 1989]

§ 54.05-10   Certification of material toughness tests.

(a) Plate material. The manufacturer of plates may certify such material, provided it has been given an appropriate heat-treatment, by reporting the results of tests of one set of Charpy impact specimens or of two drop weight specimens, as applicable, taken from each plate as rolled. Impact specimens shall be taken as outlined in section 12 of ASTM A 20 (incorporated by reference, see §54.01–1). The long axis of the Charpy specimen must be perpendicular to the final direction of rolling. When the direction of maximum stress is unknown, the manufacturer may certify on the basis of specimens taken parallel to the final direction of rolling.

(b) Pipe or tube material. (1) The manufacturer of pipe, tube, or welded fittings formed from pipe or tube may certify such material by reporting the results of tests of one set of Charpy impact specimens, provided the requirement for production in this paragraph (b)(1) or paragraph (b)(2) of this section, as well as the requirement for sampling in paragraph (b)(3) of this section are met. The specimens shall have the major axis parallel to the length of pipe or tube. In the case of welding fittings, the specimens may be taken from the tubing prior to forming provided the fittings are normalized after forming. Such specimens shall be normalized before testing.

(2) One set of specimens may represent each five (5) short tons, or less, of the pipe, tubes, or welding fittings produced from one heat of steel poured from a single melting furnace charge and subsequently processed in the same manner, provided all are given a normalizing heat-treatment in a continuous treating furnace in which the temperature is automatically controlled and checked by recording pyrometer.

(3) One set of specimens may represent each five (5) short tons, or less, of the pipe, tubes, or welding fittings that have been given a normalizing heat-treatment as a single charge in a batch-treating furnace equipped with recording pyrometer provided all have been produced from a single melting furnace heat and are subsequently processed in the same manner. If more than one melting furnace heat is present in the batch heat-treating furnace, means of identification shall be provided and one set of specimens shall be taken from each heat.

(4) One set of impact specimens shall be taken from one pipe or tube picked at random from each heat or furnace batch or portion thereof to be certified.

(c) Forgings and forged or rolled fittings. (1) The manufacturer of forgings for any purpose may certify them by reporting the results of tests of one set of Charpy impact specimens or two drop-weight specimens, as applicable, taken from each 5 short tons of product from each melting heat provided the requirements in this paragraph for production and sampling are met.

(2) One or more test blocks shall be cut from billets or blooms selected at random from each heat of material. Each test block shall be forge-reduced in thickness to the thickness of the finished forgings to be certified, within the limitations set below. After forging to the reduced thickness, the test block shall be heat-treated in the same manner as the finished forgings represented, which heat-treatment of test blocks may be carried out in the furnace with the forgings, or separately. If carried out separately, both heat-treatments shall be done in automatically controlled furnaces equipped with calibrated recording pyrometers, the certified records of which shall be made available to the inspector.

(3) One set of Charpy impact specimens or two drop-weight specimens, as applicable, shall be cut from each such test block and these specimens shall represent all forgings (up to 5 short tons) that are from the same heat of material and given the same heat-treatment as the test block, and the thickness of which does not differ from that of the test block by more than plus or minus 50 percent of 11/2 inches, whichever is less, except that forged flanges and tube sheets thicker than 51/2 inches may be qualified from a 4-inch test block.

(4) As many test blocks shall be made as are required under the foregoing rule in paragraph (c)(3) of this section to cover the weight of product and range of thickness found in the forgings represented. The major axis of the test specimens shall be parallel to the length of the test block.

(d) Bars and shapes, rolled or forged. (1) The manufacturer of forged or rolled bars and shapes may certify such by reporting the results of one set of Charpy impact specimens, or two drop-weight specimens, as applicable, produced from each 5 short tons from a single melting furnace heat, processed in a similar manner and heat-treated as a single furnace batch, if heat-treated. The impact specimens shall be cut from the heaviest section, clear of fillets, of the shape being tested with the axis of the specimens parallel to the axis of the bar or shape.

(e) Castings. (1) The manufacturer of castings may certify them by reporting the results of one set of Charpy impact specimens or two drop-weight specimens, as applicable, taken from each 5 short tons of product from each melting furnace heat. These specimens shall be taken either directly from a production casting or from test coupons cast attached thereto provided the additional requirements in this paragraph are met.

(2) One set of Charpy impact or two drop-weight specimens may represent all castings (up to 5 short tons) that are from the same heat of material and that have a thickness that does not differ from the thickness of the section from which the specimens were taken by more than plus or minus 25 percent, or 11/2 inches, whichever is less. A wider range of thicknesses from one heat may be covered by taking additional sets of specimens from thicker or thinner material as may be required.

(3) The test specimens shall be heat-treated in the same manner as the castings represented, which heat-treatment of specimens may be carried out in the furnace with the castings represented, or separately, but if carried out separately both heat-treatments shall be done in automatically controlled furnaces equipped with calibrated recording pyrometers, the certified records of which shall be made available to the marine inspector.

(f) Small parts. The manufacturer of small parts, either cast or forged, may certify a lot of not more than 20 duplicate parts or 5 short tons, whichever is less, by reporting the results of one set of Charpy impact specimens, or two drop-weight specimens, as applicable, taken from one such part selected at random, provided the same kind of material and the same process of production were used for all of the lot. When the part is too small to provide the specimens of at least minimum size, no impact test need be made. For such parts too small to impact test, toughness qualifications shall be determined by the Commandant based on material, chemical, and mechanical properties.

[CGFR 68–82, 33 FR 18828, Dec. 18, 1968, as amended by CFR 73–254, 40 FR 40164, Sept. 2, 1975; USCG–1999–5151, 64 FR 67178, Dec. 1, 1999]

§ 54.05-15   Weldment toughness tests—procedure qualifications.

(a) Plate for which Charpy V-notch impact testing is required in the parent material and for which V-notch minima are specified shall similarly have welding procedures qualified for toughness by Charpy V-notch testing. For these tests, the test plates shall be oriented with their final rolling direction parallel to the weld axis (i.e., so that transverse impact specimens result), and with the V-notch normal to the plate surface. The sample weld joint preparation shall be the same as that used in production. The number of test specimens and the location of their notches shall be as shown in Figure 54.05–15(a) and as described in paragraphs (a) (1) through (5) of this section.

(1) Three specimens with the notch centered in the weld metal.

(2) Three specimens with the notch centered on the fusion line between parent plate and weld. (The fusion line may be identified by etching the specimen with a mild reagent.)

(3) Three specimens with the notch centered in the heat affected zone, 1 mm from the fusion line.

(4) Same as paragraph (a)(3) of this section, but 3 mm from the fusion line.

(5) Same as paragraph (a)(3) of this section, but 5 mm from the fusion line.

Figure 54.05–15(a)—Charpy V-notch specimen removal details

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(b) Plate materials for which Charpy V-notch minimums are not specified, or for which a Charpy V-notch correlation with NDT is not known, and which are themselves tested for toughness by the drop-weight procedure, shall have welding procedures similarly qualified by the drop-weight test. For such qualifications, two drop-weight specimens are to be tested, with the notch positioned directly above and parallel to the centerline of the weld.

(c) Piping welding toughness tests shall be qualified, by making Charpy V-notch impact tests as prescribed in paragraph (a) of this section.

(d) Materials which are specially approved based on toughness criteria or tests, other than those discussed in paragraphs (a) and (b) of this section, shall have welding procedures tested and qualified for toughness as deemed appropriate and necessary by the Commandant.

(e) In the case of stainless steels, weld procedure toughness tests may be limited to weld metal only if this is all that is required by §54.25–15.

§ 54.05-16   Production toughness testing.

(a) For vessels of welded construction, production toughness test plates shall be prepared for each 50 feet of longitudinal and circumferential butt weld in each Class I-L vessel, or for each 150 feet in each Class II-L vessel, except for material other than stainless steel that is exempted from impact test requirements by this subchapter. In the case of stainless steels, weld production toughness tests may be limited to weld metal only if this is all that is required be §54.25–15. The test-plate thickness shall be the same as that of the vessel wall at the location of the production weld being sampled. The test plates shall be prepared, wherever possible, as run-off tabs attached at the ends of weld butts or seams. The rolling direction of the run-off tabs should be oriented parallel to the rolling direction of the adjacent production material. The test-plate material shall be taken from one of the heats of material used in the vessel, and both the electrodes and welding procedures shall be the same as used in the fabrication of the vessel. From each test plate, one set of three Charpy impact bars or two drop-weight specimens, as applicable according to the test used in procedure qualification, shall be taken transverse to the weld axis. For Charpy V-notch specimens, the notch shall be normal to the material surface and its location alternated (approximately) on successive tests between the weld metal and heat affected zone. Thus, approximately half of all weld production impact tests will be of weld metal and half of heat affected zone material. For the weld metal tests, the V-notch is to be centered between the fusion lines. For the heat affected zone tests, the notch is to be centered so as to sample, as nearly as practicable, the most critical location for toughness observed in the weld procedure qualification tests. Where the drop weight specimen is used in production weld testing, it shall be prepared in the same manner as specified for procedure qualification testing, §54.05–15(b).

(b) For vessels not exceeding 5 cubic feet in volume, one set of impact specimens, or two drop-weight specimens, as applicable according to the test used in procedure qualification, may represent all vessels from the same heat of material not in excess of 100 vessels, or one heat-treatment furnace batch. In addition, when such vessels are welded, one weld test plate made from one of the heats of material used, and two sets of impact specimens or two drop-weight specimens, as applicable, cut therefrom, may represent the weld metal in the smallest of: One lot of 100 vessels or less; or each heat-treatment furnace batch; or each 50 feet of welding for Class I-L vessels; or each 150 feet of welding for Class II-L vessels.

(c) For several vessels or parts of vessels being welded in succession, the plate thickness of which does not vary by more than one-fourth inch, and which are made of the same grade of material, a test plate shall be furnished for each 50 feet of welding for Class I-L vessels or 150 feet of welding for Class II-L vessels. For each 50- or 150-foot increment of weld, as applicable, the test plates shall be prepared at the time of fabrication of the first vessel involving that increment.

(d) The test plates and any other test material from which toughness test specimens are cut shall be given the same heat-treatment as the production material they represent. Test specimens representing other material than the weld toughness test plates shall preferably be cut from a part of the vessel material but may be cut from like material that has been heat-treated within the temperature range specified by the producer in treating the actual vessel material.

(e) For nonpressure vessel type tanks and associated secondary barriers, as defined in §38.05–4, subchapter D (Tank Vessels) of this chapter, production toughness test plates shall be prepared in accordance with paragraphs (a) and (d) of this section. One set of toughness test plates shall be prepared for each 165 feet (50 meters) of production butt type welds.

§ 54.05-17   Weld toughness test acceptance criteria.

(a) For Charpy V-notch impact tests the energy absorbed in both the weld metal and heat affected zone impact tests in weld qualification and production shall be:

(1) For weld metal specimens, not less than the transverse values required for the parent material.

(2) For heat affected zone specimens, when the specimens are transversely oriented, not less than the transverse values required for the parent material.

(3) For heat affected zone specimens, when the specimens are longitudinally oriented, not less than 1.5 times the transverse values required for the parent material.

(b) For drop-weight tests both specimens from each required set shall exhibit a no-break performance.

[CGFR 68–82, 33 FR 18828, Dec. 18, 1968, as amended by CGD 73–254, 40 FR 40164, Sept. 2, 1975]

§ 54.05-20   Impact test properties for service of 0 °F and below.

(a) Test energy. The impact energies of each set of transverse Charpy specimens may not be less than the values shown in Table 54.05–20(a). Only one specimen in a set may be below the required average and the value of that specimen must be above the minimum impact value permitted on one specimen only. See §54.05–5(c) for retest requirements.

          Table 54.05-20(a)_Charpy v-notch impact requirements------------------------------------------------------------------------                                      Minimum impact                                      value required     Minimum impact                                      for average of    value permitted         Size of specimen             each set of 3     on one specimen                                     specimens foot-     only of a set,                                        pounds \1\        foot-pounds------------------------------------------------------------------------10 x 10 mm........................               20.0               13.510 x 7.5 mm.......................               16.5               11.010 x 5 mm.........................               13.5                9.010 x 2.5 mm.......................               10.0               6.5------------------------------------------------------------------------\1\ Straight line interpolation for intermediate values is permitted.

(b) Transversely oriented Charpy V-notch impact specimens of ASTM A 203 (incorporated by reference, see §54.01–1) nickel steels must exhibit energies not less than the values shown in §54.05–20 (a). Requirements for 9 percent nickel steels are contained in §54.25–20. Other nickel alloy steels, when specially approved by the Commandant, must exhibit a no-break performance when tested in accordance with the drop weight procedure. If, for such materials, there are data indicating suitable correlation with drop-weight tests, Charpy V-notch tests may be specially considered by the Commandant in lieu of drop-weight tests. If the drop-weight test cannot be performed because of material thickness limitations (less than one-half inch), or product shape, or is otherwise inapplicable (because of heat treatment, chemistry etc.) other tests or test criteria will be specified by the Commandant.

(c) Where sufficient data are available to warrant such waiver, the Commandant may waive the requirements for toughness testing austenitic stainless steel materials. Where required, austenitic stainless steels are to be tested using the drop-weight procedure and must exhibit a no-break performance. Where data are available indicating suitable correlation of Charpy V-notch results with drop-weight NDT or no-break performance, Charpy V-notch tests may be specially considered by the Commandant in lieu of dropweight tests. If the dropweight test cannot be performed because of material thickness limitations (less than one-half inch), or product shape, or is otherwise inapplicable (because of heat treatment, chemistry, etc.) other tests and/or test criteria will be specified by the Commandant.

[CGD 73–254, 40 FR 40164, Sept. 2, 1975, as amended by USCG–2000–7790, 65 FR 58460, Sept. 29, 2000]

§ 54.05-25   [Reserved]

§ 54.05-30   Allowable stress values at low temperatures.

(a) The Coast Guard will give consideration to the enhanced yield and tensile strength properties of ferrous and nonferrous materials at low temperature for the purpose of establishing allowable stress values for service temperature below 0 °F.

(b) The use of such allowable stress values must be specially approved by the Coast Guard for each application. Further information may be obtained by writing to the Coast Guard (G-MSE).

(c) Submittals must include information and calculations specified by the Coast Guard (G-MSE) to demonstrate that the allowable stress for the material cannot be exceeded under any possible combination of vessel loads and metal temperature.

[CGD 73–133R, 39 FR 9179, Mar. 8, 1974, as amended by CGD 82–063b, 48 FR 4781, Feb. 3, 1983; CGD 95–072, 60 FR 50462, Sept. 29, 1995; CGD 96–041, 61 FR 50727, 50728, Sept. 27, 1996]

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